Impressions from the Laboratories
Electrochemistry
Various potentiostats for electrochemical measurements including cyclic voltammetry, chronoamperometry, impedance spectroscopy and much more.
Rotating Ring Disk Electrode (RRDE)
A rotating ring disk electrode used for hydrodynamic voltammetry. In particular, this system is used to investigate reaction mechanisms for specific electrochemical reactions such as the oxygen reduction reaction (ORR).
IVIUM Technologies
Analytical Measurements
FTIR-ATR Spectrometer
FTIR spectrometer for material characterisation to identify unique IR signatures and chemical bonds.
Perkin Elmer Spectrum Two
Infared Spectrometer
FTIR spectrometer fitted with a PIKE Jackfish electrochemical set-up for in-situ FTIR measurement for mechanistic insights.
Bruker Vertex 80
Electrochemical Mass Spectrometry
State of the art EC-MS to identify reaction intermediates during electrochemical reactions.
SpectroInlets
Temperature Programmed Desorption
Thermal desorption spectroscopy used to study the desorption of reactants from the surface of electrocatalytic materials.
ChemBET PULSAR PR/TPD Quantachrome
Gas Chromatograph
Gas chromatography customised by Teckso GmbH for gas product analysis specifically CO2 reduction related products such as CO, CH4 and H2.
Agilent 8860
UV-Vis Spectrometer
UV-Vis spectrometer to measure the UV and visible absorbance of inorganic and organic compounds. In addition, this instrument is used for calorimetric detection methods.
Agilent Cary 60
Vibrating Sample Magnetometer
A vibrating sample magnetometry used to measure the magnetic properties of materials including thin films and semiconductors.
Quantum Design Europe PPMS
SEM / EDS
Hitachi SU 3800 / EDAX Octane Elect Super
ICP-OES
PerkinElmer Optima 8300 DV
Headspace Gas Chromatograph
Headspace gas chromatography for detection of organic products related to various electrochemical reaction at low concentrations.
Perkin Elmer GC 2400
Single Crystal X-Ray Diffraction
Single-crystal X-ray diffractometer for structure determination at the atomic scale of crystalline solids.
Bruker kappa CCD
Powder X Ray Diffractometer
Powder X-Ray diffraction for characterisation of solid-state materials and in-situ electrochemical measurements.
Stoe STADI P Mythen
Synthesis and Preparation
Microwave
Microwave reactor for the synthesis of various materials included molecular complexes, MOFs and other solid-state materials.
Anton Parr Monowave 400 Reactor
Glove Box
Glove box used for inert chemistry including running air and moisture sensitive electrochemical reactions as well as material preparation.
MBraun labmaster 130
Laboratory Ovens/Furnaces
Vacuum Oven
Vacuum oven used for the drying of electrodes and materials.
Heraeus vacutherm
Tube furnace
Tube furnace for high-temperature synthesis of various catalysts and solid-state materials.
Thermo Scientific Lindberg Blue M