Impressions from the Laboratories

Electrochemistry

Biologic and PalmSens Potentiostat

Biologic and PalmSens Potentiostat

Electrochemistry 2
© AK Kornienko

Biologic and PalmSens Potentiostat

Electrochemistry 3
© AK Kornienko

Various potentiostats for electrochemical measurements including cyclic voltammetry, chronoamperometry, impedance spectroscopy and much more.

Biologic and PalmSens Potentiostat

Potentiostat for electrochemical measurements including cyclic voltammetry, chronoamperometry, impedance spectroscopy and much more.

Rotating Ring Disk Electrode (RRDE)

Electrochemistry 6
© AK Kornienko

A rotating ring disk electrode used for hydrodynamic voltammetry. In particular, this system is used to investigate reaction mechanisms for specific electrochemical reactions such as the oxygen reduction reaction (ORR).

IVIUM Technologies

Analytical Measurements

FTIR-ATR Spectrometer

Analytical Measurement 1 - FTIR-ATR
© AK Kornienko

FTIR spectrometer for material characterisation to identify unique IR signatures and chemical bonds.

Perkin Elmer Spectrum Two

Infared Spectrometer

Analytical Measurement 2 - In Situ Infrared
© AK Kornienko

FTIR spectrometer fitted with a PIKE Jackfish electrochemical set-up for in-situ FTIR measurement for mechanistic insights.

Bruker Vertex 80

Electrochemical Mass Spectrometry

Analytical Measurement 3 - Electrochemical Mass Spectroimetry
© AK Kornienko

State of the art EC-MS to identify reaction intermediates during electrochemical reactions.

SpectroInlets

Temperature Programmed Desorption

Analytical Measurement 4 - Temperature Programmed Desorption
© AK Kornienko

Thermal desorption spectroscopy used to study the desorption of reactants from the surface of electrocatalytic materials.

ChemBET PULSAR PR/TPD Quantachrome

Gas Chromatograph

Analytical Measurement 5 - Gas Chromotography
© AK Kornienko

Gas chromatography customised by Teckso GmbH for gas product analysis specifically CO2 reduction related products such as CO, CH4 and H2.

Agilent 8860

UV-Vis Spectrometer

Analytical Measurement 6 - UV-Vis Absorbance
© AK Kornienko

UV-Vis spectrometer to measure the UV and visible absorbance of inorganic and organic compounds. In addition, this instrument is used for calorimetric detection methods.

Agilent Cary 60

Vibrating Sample Magnetometer

Analytical Measurement 7 - Vibrating Sample Magnetometer
© AK Kornienko

A vibrating sample magnetometry used to measure the magnetic properties of materials including thin films and semiconductors.

Quantum Design Europe PPMS

SEM / EDS

Analytical Measurement 8 - SEM + EDS.jpg
© AK Kornienko

Hitachi SU 3800 / EDAX Octane Elect Super

 ICP-OES

Analytical Measurement 9 - ICP-OES
© AK Kornienko

PerkinElmer Optima 8300 DV

Headspace Gas Chromatograph

Analytical Measurement 10 - Headspace Gas Chromatography.jpg
© AK Kornienko

Headspace gas chromatography for detection of organic products related to various electrochemical reaction at low concentrations.

Perkin Elmer GC 2400

Single Crystal X-Ray Diffraction

Analytical Measurement 11 - Single Crystal XC Ray Diffraction
© AK Kornienko

Single-crystal X-ray diffractometer for structure determination at the atomic scale of crystalline solids.

Bruker kappa CCD

Powder X Ray Diffractometer

Analytical Measurement 12 - Powder X Ray Diffraction
© AK Kornienko

Powder X-Ray diffraction for characterisation of solid-state materials and in-situ electrochemical measurements.

Stoe STADI P Mythen

Synthesis and Preparation

Microwave

Synthesis and Preparation 1 - Microwave
© AK Kornienko

Microwave reactor for the synthesis of various materials included molecular complexes, MOFs and other solid-state materials.

Anton Parr Monowave 400 Reactor

Glove Box

Synthesis and Preparation 2 - Glove Box
© AK Kornienko

Glove box used for inert chemistry including running air and moisture sensitive electrochemical reactions as well as material preparation.

MBraun labmaster 130

Laboratory Ovens/Furnaces

Vacuum Oven

Laboratory Ovens, Furnaces 1.jpg
© AK Kornienko

Vacuum oven used for the drying of electrodes and materials.

Heraeus vacutherm

Tube furnace

Laboratory Ovens, Furnaces 2
© AK Kornienko

Tube furnace for high-temperature synthesis of various catalysts and solid-state materials.

Thermo Scientific Lindberg Blue M

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